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セルロースを無水酢酸でアセチル化して、セルロース中のβ-グルコース単位中の2,3,6位のOH基をアセチル基にかえたトリアセチルセルロースを合成する。これを加水分解してジアセチルセルロースにしたのち、アセトンに溶かして細孔から押し出して紡糸すると半合成繊維のアセテート繊維になる。
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